Comparison of the shear bond strength of self-adhesive resin cements to enamel and dentin with different protocol of application

Authors

  • Najmeh Ojrati Postgraduate Student of Operative Dentistry, School of Dentistry, Mashhad University of Medical Sciences, Mashhad, Iran

Keywords:

Dentin, Dental porcelain, Resin cement

Abstract

Aim: The aim of the present study was to determine the shear bond strength of self-adhesive resin cements to enamel and dentin with and without surface treatments, and compare them with conventional resin cement as the control group.

Methods: In this experimental study, buccal and lingual surface of the thirty sound human premolars were polished in order to obtain a flat surface of enamel (E) in buccal, and dentin (D) in lingual. Sixty feldspathic ceramic blocks (2×3×3 mm) were prepared and randomly divided into six groups (n=10). Each block was cemented to the prepared surface (30 enamel and 30 dentin surface) according to different protocol: E1 and D1;  RelyX ARC as control group, E2, D2; RelyX Unicem, E3, D3; acid etching +RelyX Unicem. The specimens were termocycled and subjected to shear forces by a universal testing machine at a cross head speed of 0.5 mm/min. The mode of fracture were evaluated by stereomicroscope. Data were analyzed with descriptive statistical methods using SPSS version 15. One-way ANOVA, and post hoc Tukey tests were used to compare bond strengths between the groups with different adhesives at α=0.05.

Results: Statistical analysis showed no significant differences within the enamel subgroups, but there were significant differences within the dentinal subgroups, and statistically significant differences were found between the groups D1and D3 (p=0.02). Comparison between similar enamel and dentinal subgroups showed that there was a significant difference just between the subgroups E3 and D3 (p=0.01). 

Conclusion: Elective etching of enamel did not lead to significant increase in the shear bond strength of RelyX Unicem in comparison to RelyX ARC. On the other hand, elective etching of dentin reduces the bond strength of RelyX Unicem with the dentin.

References

Torres CR, Pinto LQ, Leonel AG, Pucci CR, Borges AB. Interaction between total-etch and self-etch

adhesives and conventional and self-adhesive resin cements. Braz J Oral Sci. 2007; 6: 1376-82.

Ariki EK, Pavanelli CA, Tomm A, Zogheib LV. Cementation of ceramics and indirect composite resin to

enamel and dentin using different resin-based cements - Shear bond strength. RFO Passo Fundo. 2012; 17:

-7.

Hikita K, Van Meerbeek B, De Munck J, Ikeda T, Van Landuyt K, Maida T, et al. Bonding effectiveness of

adhesive luting agents to enamel and dentin. Dent Mater. 2007; 23(1): 71-80. doi:

1016/j.dental.2005.12.002. PMID: 16426673.

Albaladejo A, Osorio R, Toledano M, Ferrari M. Hybrid layers of etch-and-rinse versus self-etching

adhesive systems. Med Oral Patol Oral Cir Bucal. 2010; 15(1): e112-8. PMID: 19767690.

De Munck J, Van Landuyt K, Peumans M, Poitevin A, Lambrechts P, Braem M, et al. A critical review of

the durability of adhesion to tooth tissue: Methods and results. J Dent Res. 2005; 84(2): 118-32. doi:

1177/154405910508400204. PMID: 15668328.

Swartz ML, Philip RW, Day R, Johnston JF. A laboratory and clinical investigation of certain resin

restorative and cementing materials. Part 1. In vitro tests on adhesive characteristics. J Prosthet Dent. 1955;

(5): 698–704. doi: 10.1016/0022-3913(55)90098-6.

Zorzin J, Petschelt A, Ebert J, Lohbauer U. pH neutralization and influence on mechanical strength in self- adhesive resin luting agents. Dent Mater. 2012; 28(6): 672–9. doi: 10.1016/j.dental.2012.03.005. PMID:

Monticelli F, Osorio R, Mazzitelli C, Ferrari M, Toledano M. Limited decalcification/diffusion of self- adhesive cements into dentin. J Dent Res. 2008; 87(10): 974-9. doi: 10.1177/154405910808701012. PMID:

Cantoro A, Goracci C, Papacchini F, Mazzitelli C, Fadda GM, Ferrari M. Effect of pre-cure temperature on

the bonding potential of self-etch and self-adhesive resin cements. Dent Mater. 2008; 24(5): 577–83. doi:

1016/j.dental.2007.06.012. PMID: 17659770.

De Munck J, Vargas M, Van Landuyt K, Hikita K, Lambrechts P, Van Meerbeek B. Bonding of an auto- adhesive luting material to enamel and dentin. Dent Mater. 2004; 20(10): 963–71. doi:

1016/j.dental.2004.03.002. PMID: 15501325.

Abo-Hamar SE, Hiller KA, Jung H, Federlin M, Friedl KH, Schmalz G. Bond strength of a new universal

self-adhesive resin luting cement to dentin and enamel. Clin Oral Investig. 2005; 9(3): 161–7. doi:

1007/s00784-005-0308-5. PMID: 15856343.

Fabianelli A, Goracci C, Bertelli E, Monticelli F, Grandini S, Ferrari M. In vitro evaluation of wall-to-wall

adaptation of a self-adhesive resin cement used for luting gold and ceramic inlays. J Adhes Dent. 2005; 7:

–40. PMID: 15892362.

Behr M, Rosentritt M, Regent T, Lang R, Handel G. Marginal adaptation in dentin of a self-adhesive

universal resin cement compared with well-tried system. Dent Mater. 2004; 20(2): 191–7. doi:

1016/S0109-5641(03)00091-5. PMID: 14706803.

Moura SK, Pelizzaro A, Dal Bianco K, de Goes MF, Loguercio AD, Reis A, et al. Does the acidity of self- etching primers affect bond strength and surface morphology of enamel? J Adhes Dent. 2006; 8(2): 75–83.

PMID: 16708718.

Pashley DH, Tay FR. Aggressiveness of contemporary self-etching adhesives. Part II: etching effects on

unground enamel. Dent Mater. 2001; 17(5): 430–44. doi: 10.1016/S0109-5641(00)00104-4. PMID:

Van Meerbeek B, Kanumilli P, De Munck J, Van Landuyt K, Lambrechts P, Peumans M. A randomized

controlled study evaluating the effectiveness of a two-step self-etch adhesive with and without selective

phosphoric-acid etching of enamel. Dent Mater. 2005; 21(4): 375–83. doi: 10.1016/j.dental.2004.05.008.

PMID: 15766585.

Van Landuyt KL, Peumans M, De Munck J, Lambrechts P, Van Meerbeek B. Extension of a one-step self- etch adhesive into a multi-step adhesive. Dent Mater. 2006; 22(6): 533–44. doi:

1016/j.dental.2005.05.010. PMID: 16300826.

Perdigao J, Anauate-Netto C, Carmo AR, Lewgoy HR, Cordeiro HJ, Dutra-Correa M, et al. Influence of

acid etching and enamel bevelling on the 6-month clinical performance of a self-etch dentin adhesive.

Compend Contin Educ Dent. 2004; 25(1): 33-4. PMID: 15645878.

Shinchi MJ, Soma K, Nakabayashi N. The effect of phosphoric acid concentration on resin tag length and

bond strength of a photo-cured resin to acid-etched enamel. Dent Mater. 2000; 16(5): 324–9. doi:

1016/S0109-5641(00)00024-5. PMID: 10915893.

Shiu P, De Souza-Zaroni WC, Eduardo Cde P, Youssef MN. Effect of feldspathic ceramic surface

treatments on bond strength to resin cement. Photomed Laser Surg. 2007; 25(4): 291-6. doi:

1089/pho.2007.2018. PMID: 17803387.

Da Silva Ferreira S, Hanashiro FS, de Souza-Zaroni WC, Turbino ML, Youssef MN. The porcelain surf

Influence of aluminum oxide sandblasting associated with Nd:YAG or Er:YAG lasers on shear bond

strength of a feldspathic ceramic to resin cements. Photomed Laser Surg. 2010; 28(4): 471-5. doi:

1089/pho.2009.2528. PMID: 19780632.

Pekperdahci T, Turkoz Y, Ozan O, Seker E. The effects of different adhesive agents on the shear bond

strength of a self-adhesive resin cement. J Appl Biomater Funct Mater. 2012; 10(2): 149-56. doi:

5301/JABFM.2012.9255. PMID: 22798242.

Vaz RR, Hipólito VD, D'Alpino PH, Goes MF. Bond strength and interfacial micromorphology of etch- and-rinse and self-adhesive resin cements to dentin. J Prosthodont. 2012; 21(2): 101-11. doi:

1111/j.1532-849X.2011.00794.x. PMID: 22044733.

Viotti RG, Kasaz A, Pena CE, Alexandre RS, Arrais CA, Reis AF. Microtensile bond strength of new self- adhesive luting agents and conventional multistep systems. J Prosthet Dent. 2009; 102(5): 306-12. doi:

1016/S0022-3913(09)60180-3. PMID: 19853172.

Saskalauskaite E, Tam LE, McComb D. Flexural strength, elastic modulus, and pH profile of self-etch resin

luting cements. J Prosthodont. 2008; 17(4): 262-8. doi: 10.1111/j.1532-849X.2007.00278.x. PMID:

De Munk J, Vargas M, Van Landuyt K, Hikita K, Lambretchts, Van Meerbeek B. Bonding of an auto- adhesive luting material to enamel and dentin. Dent Mat. 2004; 20: 963-71. doi:

1016/j.dental.2004.03.002. PMID: 15501325.

Barcellos DC, Batista GR, Silva MA, Rangel PM, Torres CR, Fava M. Evaluation of Bond Strength of

Self-adhesive Cements to Dentin With or Without Application of Adhesive Systems. J Adhes Dent. 2011;

(3): 261-5. doi: 10.3290/j.jad.a19224. PMID: 21734960.

Aschenbrenner CM, Lang R, Handel G, Behr M. Analysis of marginal adaptation and sealing to enamel

and dentin of four self-adhesive resin cements. Clin Oral Investig. 2012; 16(1): 191-200. doi:

1007/s00784-010-0501-z. PMID: 21327799.

Hickel R, Roulet JF, Bayne S, Heintze D, Mjor IA, Peters M, et al. Recommendations for conducting

clinical studies of dental restorative materials. Science Committee Project 2/98--FDI World Dental

Federation study design (Part I) and criteria for evaluation (Part II) of direct and indirect restorations

including onlays and partial crowns. J Adhes Dent. 2007; 9: 121-47. PMID: 18341239.

Rosentritt M, Behr M, Lang R, Handel G. Influence of cement type on the marginal adaptation of all- ceramic MOD inlays. Dent Mater. 2004; 20(5): 463-9. doi: 10.1016/j.dental.2003.05.004. PMID:

Ibarra G, Johnson GH, Geurtsen W, Vargas MA. Microleakage of porcelain veneer restorations bonded to

enamel and dentin with a new self-adhesive resin-based dental cement. Dent Mater. 2007; 23(2): 218-25.

doi: 10.1016/j.dental.2006.01.013. PMID: 16499961.

Sarr M, Mine A, De Munck J, Cardoso MV, Kane AW, Vreven J, et al. Immediate bonding effectiveness of

contemporary composite cements to dentin. Clin Oral Investig. 2010; 14(5) 569-577. doi: 10.1007/s00784- 009-0327-8. PMID: 19705169.

Abo-Hamar SE, Hiller KA, Jung H, Federlin M, Friedl KH, Schmalz G. Bond strength of a new universal

self-adhesive resin luting cement to dentin and enamel. Clin Oral Investig. 2005; 9(3): 161-7. doi:

1007/s00784-005-0308-5. PMID: 15856343.

Peutzfeldt A, Sahafi A, Flury S. Bonding of Restorative Materials to Dentin with Various Luting Agents.

Oper Dent. 2011; 36(3): 266-73. doi: 10.2341/10-236-L. PMID: 21740244.

Pereira PNR, Okuda M, Sano H, Yoshikawa T, Burrow MF, Tagami J. Effect of intrinsic wetness and

regional difference on dentin bond strength. Dent Mater. 1999; 15(1): 46-53. doi: 10.1016/S0109- 5641(99)00013-5. PMID: 10483395.

Yoshikawa T, Sano H, Burrow MF, Tagami J, Pashley DH. Effects of dentin depth and cavity

configuration on bond strength. J Dent Res. 1999; 78(4): 898–905. doi: 10.1177/00220345990780041001.

PMID: 10326734.

Nakabayashi N, Watanabe A, Arao T. A tensile test to facilitate identification of defects in dentin bonded

specimens. J Dent. 1998; 26(4): 379–85. doi: 10.1016/S0300-5712(97)00021-3. PMID: 9611944.

Hashimoto M, Ohno H, Kaga M, Sano H, Tay FR, Oguchi H, et al. Over-etching effects on micro-tensile

bond strength and failure patterns for two dentin bonding systems. J Dent. 2002; 30(2-3): 99-105. doi:

1016/S0300-5712(02)00004-0. PMID: 12381409.

Published

2022-01-18

Issue

Section

Articles